Describes the preparation of 3-carbethoxycoumarin 4, a fused-ring heterocycle.
1,242 words (approx. 5 pages) |
3 sources |
2001
From the Paper:
"The reaction of salicylaldehyde 1 with diethyl malonate 2 was reacted in a basic environment with piperidine 3. The reaction was a base catalysed condensation which also involved a transesterification step to produce 3-carbethoxycoumarin 4. The purification of 3-carbethoxycoumarin 4 was achieved through filtration. The experiment was successful with the product being identified as 3-carbethoxycioumarin 4; it was identified as such through its' melting point, IR, 1H NMR, and 13C NMR."
More papers on The Synthesis of 3-Carbethoxycoumarin:
The Synthesis of 3-Carbethoxycoumarin (2012, January 16). Retrieved February 13, 2012, from http://www.academon.com/Term-Paper-The-Synthesis-of-3-Carbethoxycoumarin/1964
"The Synthesis of 3-Carbethoxycoumarin" 16 January 2012. Web. 13 Feb. 2012. <http://www.academon.com/Term-Paper-The-Synthesis-of-3-Carbethoxycoumarin/1964>
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Published by:
Asj
Publisher Since:
Jul 01, 2001
I am currently going for my Ph.D. in Chemistry. With a major in medicinal Chemistry.