Describes the preparation of 3-carbethoxycoumarin 4, a fused-ring heterocycle.
Written in 2001; 1,242 words; 3 sources; $ 42.95
From the Paper:
"The reaction of salicylaldehyde 1 with diethyl malonate 2 was reacted in a basic environment with piperidine 3. The reaction was a base catalysed condensation which also involved a transesterification step to produce 3-carbethoxycoumarin 4. The purification of 3-carbethoxycoumarin 4 was achieved through filtration. The experiment was successful with the product being identified as 3-carbethoxycioumarin 4; it was identified as such through its' melting point, IR, 1H NMR, and 13C NMR."
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